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Hi-res question

I'm pretty new to this hi-res digital audio thing so please bear with me:

A guy wants to send me a song to have me master it for him. He says that he will send it to me on a CD-R as a 32-bit float .wav file. I will be using Sonic Foundry Vegas 3.0 to master - it supports 24/96 as well as does my soundcard (DAL CardDeluxe).

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